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The reductive cycloelimination of the complexes L m (Br)MoPPh 2O (CH 2 ) n -Cl (3a,b) [n = 2 (a), 3 (b); L m Mo = η 5 -C 5 H 5 Mo(CO) 2 ], which can be obtained from the reaction of PPh 2 O-(CH 2 ) n -Cl (1a, b) and L m (Br)MoCO (2) in n-hexane/THF, results in the formation o f the metallacycles(4a,b). Compared withthe five-membered heterocycle 4a is thermally more stable.

zeitschrift für naturforschung b

Notizen: Darstellung und Eigenschaften von und Reaktionen mit metallhaltigen Heterocyclen, XXXVIII [1] Fünf- und sechsgliedrige Oxaphosphamolybdacycloalkane durch reduktive Cycloeliminierung/Preparation and Properties of, and Reactions with, Metal-Containing Heterocycles, XXXVIII [1] Five- and Six-Membered Oxaphosphamolybdacycloalkanes by Reductive Cycloelimination