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has been subjected to single-crystal x-ray diffraction analyses at -21° and -139 °C (orthorhombic,  Pnma, Z  = 4,  -139 °C:  a =  1150.9(3);  b =  1136.8(2) ; c = 651.6(2) pm). The molecules adopt  the antiperiplanar conformation with the crystallographically imposed symmetry m (C s ) and are  aligned in extended linear antimony chains with short intermolecular contacts (-139 °C: Sb-Sb  283.8(1), Sb···Sb 367.8(1) pm; Sb-Sb---Sb 179.2°). The structure is compared with those of  similar compounds.

zeitschrift für naturforschung b

Element—Element-Bindungen, III [1]. Intermolekulare Sb···Sb-Wechselwirkungen im kristallinen Tetramethyldistiban 1  / Element—Element Bonds, III [1]. Intermolecular Sb···Sb Interactions in Crystalline Tetramethyldistibane