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The title compound C 12 H 49 Cl 4 I 2 N 8 O  16 Pt 2 , Mr 1314.1, is monoclinic P 2 1  (from structural analysis), a = 8.74(1), b = 11.36(1), c = 8.63(1), β = 107.6(5), V = 817 Å 3 , Z = 1, D m  (flotation) = 2.65 g cm -3 , D c  = 2.66 g cm -3 , MoK ɑ  λ = 0.71069, μ = 110.7 cm -1 , R = 0.063 for 1068 observed reflections. Rotation photographs show diffuse patterns corresponding to odd values of k together with weak Bragg reflections. Refinement of diffractometer data was carried out in space groups Pm, P2 1 /m and P2 1 ; both refinement in Pm and P2 1  give satisfactory agreement and lead to very similar crystal structures

Structure of the Linear-Chain Mixed Valence Compound Bis(l,3-diaminopropane)platinum(II)bis(l,3-diaminopropane)- diiodoplatinum(IV)tetraperchlorate