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Alkyldifluorophosphites, ROPF 2  (R = p-substituted benzyl group, neopentyl, 1-adamantyl) have been obtained by a new method, involving reaction of the appropriate alkyl trimethylsilylether, ROSiMe 3  with chlorodifluorophosphine, PF 2 Cl. Reactions of these difluorophosphites with platinum(II) complexes of the type [L 2 PtCl 2 ] (L = PEt 3 , PPh 3 ) led to products such as trans-[L 2 PtCl(POF 2 )] and {[p-XC 6 H 4 CH 2 PPh 3 ] + } 2 [Pt(POF 2 ) 4 ] 2- , (X = H, Me, Cl, NO 2 ). The ease of carbon-oxygen cleavage in ROPF 2  is characteristically related to the nature of the leaving group, R.

A New Synthesis of Organodifluorophosphites and their Reactions with Platinum(II) Complexes