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Amidinato complexeswith sub­stituents R at the cyclopentadienyl and R′ in the p-position of the phenyl at the asym­metric C atom were synthesized and characterized. The diastereomers differing in their  1 H NMR spectra were partly separated by fractional crystallization. After equilibration with respect to the labile Mo configuration the diastereomer ratio, a measure for the asymmetric induction from the chiral ligand on the formation of the two Mo configura­tions at equilibrium, was determined by  1 H NMR integration. The diastereomer ratio decreases for substituents R′ = F and R = CH 3 , and increases for R' = OCH 3 , com­pared to the unsubstituted compound.

zeitschrift für naturforschung b

Optisch aktive Übergangsmetall-Komplexe, 84 [1] Substituenten-Effekte in Diastereomerengleichgewichten von quadratisch-pyramidalen Mo-Komplexen / Optically Active Transition Metal Complexes, 84 [1] Substituent Effects in Diastereomer Equilibria of Square-Pyramidal Mo Complexes