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Orange crystals of K 2 Ti(O 2 )F 4  · H 2 O have been obtained from aqueous solution. The crystal structure (space group P2 1 /n, a = 604.3(3), b = 1424.6(4), c = 761.0(2) pm, β = 103.98°, Z = 4, dc = 2.63 gcm -3 , d m  = 2.62 gcm -3 , R = 0.051 for 2257 independent reflections) shows isolated di(μ-fluoro)-bridged [Ti 2 (O 2 ) 2 F 8 ] 4-  anions, which are inter­connected by hydrogen bonded H 2 O forming infinite chains.

zeitschrift für naturforschung b

Peroxofluorokomplexe der Übergangsmetalle, V [1-3] Kristallstruktur von K 2 Ti(O 2 )F 4  · H 2 O (orange) mit einem Di(μ-fluoro)diperoxo-hexafluorodititanat(IV)-Anion / Transition Metal Peroxofluoro Complexes, V [1-3] Crystal Structure of K 2 Ti(O 2 )F 4  · H 2 O (orange) with a Di(μ-fluoro)diperoxo-hexafluorodititanate(IV) Anion