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The hetero metal sulfur aggregates [Co(WS 4 ) 2 ]  n-  (with variable electron population: n = 2, 3) could be isolated as salts and characterized by physical measurements (in-cluding X-ray structure analysis). Experimental and theoretical investigations show that due to a strong metal → ligand electron delocalisation WS4 2- (like MOS 4  2- ) is a non-innocent ligand and that the additional charge upon reduction is located mainly at the S atoms of the ligand system.

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Notizen: Zum Verständnis der zentralen Rolle des Schwefels in Multi-Metall-Aggregaten mit verschiedener Elektronenpopulation: [S 2 WS 2 CoS 2 WS 2 ] n-  (n = 2, 3)/On the Central Role of Sulfur in Multi Metal Aggregates with Different Electron Populations: [S 2 WS 2 CoS 2 WS 2 ] n- (n = 2, 3)