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A stereospecific synthesis of 4,8-dimethylspiro(4,5)-deca-7-ene-1,6-dione from 4,7-dimethylcoumarine in high yield is reported. The configuration of this product is established according to its  1 H NMR and  13 C NMR data.

Stereospecific Synthesis of 4,8-Dimethylspiro(4,5)-deca-7-ene-1,6-dione A Synthetic Route to the Acoranes