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The oxidative addition of Br 2  to [PtCl 4 ] 2- in HBr yields almost pure trans-[PtCl 4 Br 2 ] 2- , in HCl nearly pure [PtCl 5 Br] 2- , and in CH 2 Cl 2  by a quantitative and stereospecific reaction completely pure trans-[PtCl 4 Br 2 ] 2- . This is confirmed by ion exchange chromatography on diethylaminoethyl cellulose and by analysis of the vibrational spectra in comparison with the IR and Raman spectra of the well-known species of the series [PtCl n Br 6-n ] 2-  , n = 0-6. The literature concerning trans-[PtCl 4 Br 2 ] 2-  and other mixed ligand complexes is critically discussed.

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Darstellung von trans-[PtCl 4 Br 2 ]  2  -und [PtCl 5 Br]  2-  durch oxidative Addition an [PtCl 4 ] 2- /Preparation of trans-[PtCl 4 Br 2 ]  2- -and [PtCl 5 Br]  2 - by Oxidative Addition to [PtCl 4 ] 2-