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The crystal structures of CH 3 S-CO-CONH 2  (1), CH 3 S-CS-CONH 2  (2), C 2 H 5 O-CO-CSNH 2  (3) and K[OSC-CONH 2 ] (4) have been determined by single crystal X-ray diffraction. The molecules 1, 2 and 3 are nearly planar and form centrosymmetric dimers by N H···O or N-H···S hydrogen bonds with the amidic oxygen or sulfur atom as acceptor atoms. The anion of 4 is not quite planar. The torsional angle around the C-C bond is 18.4°. The conformations of the title compounds are E, Z' (1 and 2), Z, Z' (3) and Z (4). According to the vibrational spectra, which are discussed briefly, 1 and 3 retain their conformation also in solution.

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Molekülstrukturen, Schwingungsspektren und Konformation der Thiooxalsäurederivate CH 3 S-CO-CONH 2 , CH 3 S-CS-CONH 2 , C 2 H 5 O-CO-CSNH 2  und K[OSC-CONH 2 ] /  Molecular Structure, Vibrational Spectra and Conformation of the Thiooxalic Acid Derivatives CH 3 S-CO-CONH 2 , CH 3 S-CS-CONH 2 , C 2 H 5 O-CO-CSNH 2  and K[OSC-CONH 2 ]