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Crystal Structure, Antimonate(V) The compounds MSbsOi3 (M = H3O, Na, K) have been prepared and characterised by chemical analysis and X-ray structure determination. They are isostructural, space group Cmem, with a = 657.7(2), 657.3(2), 658.4(2); b = 887.3(3), 888.7(2), 888.2(2); c = 1682.6(5), 1651.5(3), 1677.0(3) pm for M = H30, Na, K, respectively. The polymeric structures consist of SbOß octahedra linked via edges and vertices to form an Sb50i3 framework, in which the univalent cations occupy holes. Because these ions display severe disorder, X-ray methods alone would not be sufficient to establish the chemical constitutions.

zeitschrift für naturforschung b

Darstellung und Kristallstrukturen einiger MSb 5 O 13 -Verbindungen (M = H 3 O, Na, K)/Preparation and Crystal Structure of Some MSb 5 O 13  Compounds (M = H 3 O, Na, K)