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The system TlI-Tl 2 Se was investigated by DTA, X-ray and metallographic methods. At the Tl 2 Se corner of the system a solid solution up to 25 mol% TlI is observed, which decomposes peritectically at 681 K. Two new compounds Tl 5 ISe 2  and Tl 6 I 4 Se were found. The latter is isotypic to a class of compounds found in the TlX-TI 2 S systems [2]. The crystal structure of Tl 6 Cl 4 S was determined. It is based on the TlCl structure (CsCl-type) in which 1/5 of the Tl or Cl atoms, resp., are substituted by Tl 2 S in a regular manner. The coordination of the anions (Cl, S) is very similar to the coordination of Cl in TlCl or S in Tl 2 S resp.

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Das Zustandsdiagramm Thallium(I)iodid-Thallium(I)selenid und die Kristallslruktur der Verbindungsklasse Tl 6 X 4 Y/The System Thallous Iodide -Thallous Selenide and the Structure of the Tl 6 X 4 Y Compounds