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A new synthetic method for the preparation of the geometrical isomers of (FPNBu t )2 by amine elimination from Me 2 N-P(F)-NBu t SiMe 2  is described. The  13 C,  19 F, and  31 P NMR investigations lead to new structural assignments

The Nuclear Magnetic Resonance Spectra of Geometrical Isomers of 2,4-Difluoro-l,3- di-t-butylcyclodiphosph(III)azane