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By using chemical transport reactions with various transporting agents (HgCl 2 , NbCl 5 , Nb 3 O 7 Cl) a slightly substoiehiometric NbO 2 -phase, β-NbO 2 , was obtained from samples with O/Nb ∼ 1.5 (source; T &gt; 1373 K) and with deposition temperatures &gt; 1273 K (sink). The rango of composition of β-NbO 2  was found to exist from NbO 1.990  to NbO 1.998 .

Zur Darstellung und Kristallstruktur von β-NbO 2 / Synthesis and Crystal Structure of β-NbO 2