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The phosphinothioformimidato complex(1) crystallizes triclinic in the space group P1̄ with lattice constants a = 989.4(9) pm, b - 1042.0(8) pm, c = 1088.5(8) pm, α = 91.45(4)°, β = 97.10(4)°, γ = 100.53(5)°. The four-membered chelate ringis folded over the P-S edge by a dihedral angle of 167.1°. The crystal system of the thiophosphoryl thioformimidato complex(2) is monoclinic with the space group P2 1 /c, and the lattice parameters are a = 1109.5(3) pm, b = 966.0(3) pm, c = 2256.7(3) pm, β=103.11(2)°. The chelate ligand is linked to the metal by two S atoms forming a five-membered ring in the “envelope” conformation with the thiophosphoryl S atom at the apical position.

zeitschrift für naturforschung b

Phosphinsubstituierte Chelatliganden, VI [1]. Kristallstrukturen von Tetracarbonyl(diphenylphosphino -N-phenylthioformimidato -P,S )mangan(I) und Tetracarbonyl(diphenylthiophosphoryl-N-phenylthioformimidato-S,S')mangan(I) / Phosphine Substituted Chelate Ligands, VI [1]. Crystal Structures of Tetracarbonyl(diphenylphosphino-N-phenylthioformimidato-P,S)- manganese(I) and Tetracarbonyl(diphenylthiophosphoryl-X-phenylthioformimidato-S.S')- manganese(I)