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The reaction of trans-bromotetracarbonyl(phenylcarbyne)chromium (1) with lithium phenylselenolate and subsequent protonation with aqueous hydrochloric acid leads to (CO) 5 Cr[Se 2 (C 6 H 5 ) 2 ] (3) and (CO) 4 Cr(μ-SeC 6 H 5 ) 2 Cr(CO) 4  (4). From 1 and lithium 4-methylphenylthiolate (CO) 5 CrC(C 6 H 5 )SC 6 H 4 CH 3  (5) and (CO) 5 CrS(C 2 H 5 )(4-CH 3 C 6 H 4 ) (6) are obtained, if triethyloxonium tetrafluoroborate is used instead of hydrochloric acid. The analoguous reaction of 1 with lithium phenylselenolate yields the seleno ether complex (7). Reaction conditions, properties, spectroscopic data and the results of an X-ray structure determination of the binuclear complex (4) are reported.

zeitschrift für naturforschung b

Übergangsmetall-Carbin-Komplexe, LXXII [1]. Reaktionen von trans-Bromotetracarbonyl(phenylcarbin)chrom mit Lithiumthiokresolat und Lithiumselenophenolat / Transition Metal Carbyne Complexes, LXXII [1]. Reactions of trans-Bromotetracarbonyl(phenylcarbyne)chromium with Lithium Thiocresolate and Lithium Phenylselenolate