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Crystalline CuAlCl 4  was prepared from CuCl and AlCl 3  in a quartz tube at 533 K. The crystal structure was determined [P4̄2c, a = 543.0(1), c = 1009.6(1) pm, Z = 2, R w  =0.034 for 345 reflections]. The chlorine atoms form a distorted cubic close-packed lattice, with copper and aluminium each occupying an eighth of the tetrahedral holes (site symmetries 4̄ and 222, respectively).

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Darstellung und Kristallstruktur von Kupfer(I)tetrachloroaIuminat, CUAlCl 4 / Preparation and Crystal Structure of Copper(I) Tetrachloroaluminate, CuAlCl 4