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The reaction of Re 2 (CO) 10  with LiSi(C 6 H 5 ) 3  and subsequent alkylation by (C 2 H 5 ) 3 OBF 4  yields not only (CO) 9 Re 2 C(OC 2 H 5 )Si(C 6 H 5 ) 3  but also Re 1 -ax,Re 2 -eq-[C(OC 2 H 5 )Si(C 6 H 5 ) 3 ] 2 (CO) 8 Re 2  (1). The analogous isomeric complexes Re 1 -ax-[C(OC 2 H 5 )C 6 H 4 CH 3 ]-Re 2 -eq-[C(OC 2 H 5 )Si(C 6 H 5 ) 3 ](CO) 8 Re 2  (2) and Re 1 -ax-[C(OC 2 H 5 )Si(C 6 H 5 ) 3 ]-Re 2 -eq-[C(OC 2 H 5 )C 6 H 4 CH 3 ](CO) 8 Re 2  (3) are obtained by treatment of eq- or ax-(CO) 9 Re 2 C(OC 2 H 5 )Si(C 6 H 5 ) 3  with LiC 6 H 4 CH 3  and subsequent alkylation by (C 2 H 5 ) 3 OBF 4 . Reaction conditions, and properties and spectroscopic data of the new compounds are reported

zeitschrift für naturforschung b

Übergangsmetall-Carben-Komplexe, CXXIII [1] Dicarbenoktacarbonyldirhenium-Komplexe / Transition Metal Carbene Complexes, CXXIII [1] Dicarbeneoctacarbonyldirhenium Complexes