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Tetrasulfur tetraimide reacts with (THF)M(CO) 5  (M = Cr, W) to form isolable complexes of the type (S 4 N 4 H 4 )M(CO) 5  (1) and (S 4 N 4 H 4 )[M(CO) 5 ] 2  (2) respectively,  1 H NMR and X-ray investigations show the metal to be coordinated to sulfur atoms. In solution partially dissociation of M(CO) 5  moieties is observed leading to different equilibria. They are studied by  1 H NMR

G. Schmid-R. Greese • Tetraschwefeltetraimid als Ligand in Übergangsmetallkomplexen / Tetrasulfur Tetraimide as Ligand in Transition Metal Complexes