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New methods are reported which allow the synthesis of pure UCl 5  and UCl 6  in high yields. UCl 5  is obtained by chlorination of UF 5  · 2 SbF 5  with BCl 3  at low temperatures, UCl 6  by direct chlorination of UCl 4  in SbCl 5 .

Neue effektive Synthesemethoden für UCl 5 und UCl 6 / New Effective Methods for the Synthesis of UCl 5 and UCl 6