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Products of the reaction between MBr 5  and PhLi are proved to be benzyne complexes [M(C 6 H 5 ) 4 (CeH 4 ) 2 (Li · OC 4 H 10 ) n ], (M = Nb, Ta, W). Analysis of the temperature dependent 1 H and 7 Li NMR Spectra of [Ta(C 6 H 5 ) 4 (C 6 H 4 )2(Li·OC 4 H 10 ) 3 ] are interpreted on the basis of square antiprismatic/dodecahedral structure with facial C 6 H 4  groups.

zeitschrift für naturforschung b

Übergangsmetallbenz - in-Komplexe. Dynamisches Verhalten von [Ta(C 6 H 5 ) 4 (C 6 H 4 )a(Li • OC 4 H 10 ) 3 ] / Transition Metal Benzyne Complexes. Fluxional Behaviour of [TA(C 6 H 5 ) 4 (C 6 H 4 ) 2 (Li·OC 4 H 10 ) 3 ]