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C 16 H 18 N 2· 2 C 12 H 4 N 4 , C 40 H 26 N 10 , Mr = 646.7, crystallizes in space group P1̄ with a = 6.843(2), 6 = 7.845(3), c = 16.208(7) Å, α = 84.59(3), β = 81.63(3), γ = 75.75(3)°, V = 832.9 Å 3  , Z = 1, d c  = 1.29 Mgm -3  . Final weighted R = 0.107 based on 2894 reflections. The structure consists of stacks of TCNQ π-dimers with interplanar distances of 3.25(1) Å within a dimer and 3.54(1) A between dimers. The phenazine species do not form stacks and show no electronic interaction with adjacent E 2 P or TCNQ molecules.

zeitschrift für naturforschung b

The Crystal and Molecular Structure of the 1:2 5,10-Dihydro-5,10-diethylphenazine-(E 2 P)-2,2′-(2,5-Cyclohexadiene-1,4- diylidene)bispropanedinitrile (TCNQ) Complex