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The reaction of H 2 Fe(CO) 4  with trimethylphosphite in various stoichiometric ratios is reported. The compounds H 2 Fe(CO) 2 [P(OCH 3 ) 3 ] 2  (stoichiometry of reactants 1:2), H 2 Fe(CO) 3 P(OCH 3 ) 3  (1:1), Fe 3  (CO) 11 [P(OCH 3 ) 3 ], and H 3 Fe 4  (CO) 11 [P(OCH 3 ) 2 ] (3.5:1) were obtained.

zeitschrift für naturforschung b

Substitutionsreaktionen von Tetracarbonyl(dihydrido)eisen mit Trimethylphosphit/Substitution Reactions of Tetracarbonyl(dihydro)iron with Trimethylphosphite