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Benzoato-pyridine-iodine(I) and phthalato-bis(pyridine-iodine(I)) crystallize in the monoclinic spacegroup P2 1 /c. In both cases iodine(I) shows an almost linear coordination towards the pyridine-N and one carboxylate-O donor atom. The I -N distances range from 228 to 232 pm, the I - O distances from 213 to 219 pm. The vibrational spectra contain frequencies in the range 136-145 and 164-175 cm - 1  assigned to the quasi-symmetric and quasi-antisymmetric N-I-O-vibrations. The IR and Ra spectra of the benzoate and phthalate ligands are similar to those of the crystalline benzoic and phthalic acids.

zeitschrift für naturforschung b

Kristall-und Molekülstrukturen von Benzoato-pyridin-iod(I) und Phthalato-bis(pyridin-iod(I))/ Crystal and Molecular Structures of Benzoato-pyridine-iodine(I) and Phthalato-bis(pyridine-iodine(I))