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The alkyls MR 3  (M = B, AI, Ga, In) react with pyrazine (Pz) and sodium in THF to yield persistent radical complexes Pz(MR 2 ) 2  ·  + MR 4  -  (1). Use of TIR 3  leads to rapid deposition of thallium metal. The formation of these ionic complexes 1 is the result of MR 3  dissociation into  + MR2 and -MR 4  ions. All radicals have been identified and characterized by ESR; the data reveal the influence ofback bonding in the boron derivative.

zeitschrift für naturforschung b

Koordinationsverbindungen des reduzierten Pyrazins mit Alkylderivaten von Bor, Aluminium, Gallium und Indium / Coordination Complexes of Reduced Pyrazine and Alkyl Derivatives of Boron, Aluminum, Gallium, and Indium