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The interaction of RR'N-PCl 2  (1) with LiNR"SiMe 3  gives monomeric phospha(IH)-azenes RR'N-P=N-R"; R = R"=i-C 3 H 7 , R'= (CH 3 ) 3 C (3a); R=i-C 3 H 7 ,R'=R" = (CH 3 ) 3 C (3b); R = i-C 3 H 7 , R' = (CH 3 ) 3 C, R"=(CH 3 ) 3 Si (3c) as distillable liquids. 3a adds PCl 3  with formation of RR'N-PCl-NR-PCl 2 , R = i-C 3 H 7 , R'=(CH 3 ) 3 C (6).

New Phospha(III)azenes / New Phospha(III)azenes