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Tetrafluoroborate complexes (η 5  -C 5 H 5 )Mo(CO) 2 (PR 3 )FBF 3  have been prepared by hydride abstraction from the corresponding hydrido compounds using Ph 3 CBF 4 . The tetrafluoroborate ligand in (η 5  -C 5 H 5 )Mo(CO) 2 (L)FBF 3  (L = CO, PR 3 ) is easily sub-stituted by phosphanes, cis-and trans-butene(2), a-acetamidocinnamic acid and buta-diene. Nucleophilic addition of HNMe 2  to the butadiene complex [(η 5  -C 5 H 5 )Mo(CO) 3  butadiene)] + BF 4  -  gives the β-aminoacyl chelate compound 7.

zeitschrift für naturforschung b

Metallorganische Lewissäuren, V [1] Reaktionen von Carbonyl-η 5 -cyclopentadienylmolybdä ntetrafluoroboraten (η 5 -C 5 H 5 )MO(CO) 2 (L)FBF 3  (L=CO, PR 3 ) mit Phosphanen und Alkenen / Organometallic Lewis Acids, V [1] Reactions of Carbonyl-η 5 -cyclopentadienyl Molybdenum Tetrafluoroborates (η 5 -C 5 H 5 )Mo(CO) 2 (L)FBF 3  (L = CO, PR 3 ) with Phosphanes and Alkenes