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The reaction of FeCl 3  with S 4 N 4  in CH 2 Cl 2  at room temperature yields S 6 N 4  2+ (FeCl 4  - ) 2  (A), among other products. Crystal data of A: Space group P2 1 /c, Z = 4, α = 12.090(4), b= 11.745(3), c= 13.918(3) Å, β= 101.25(2)°. In its dimensions and its conformation the S 6 N 4  2+  -cation in A agrees well with the S 6 N 4  2+  -cation in other salts. There exists one close S···Cl contact between each of the S atoms of the central S 4  ring in the cation and the neighbouring FeCl 4  -  anions (3.04 to 3.16 Å; for comparison: the S···Cl van der Waals distance is 3.50 Å).

zeitschrift für naturforschung b

S 4 N 4  und seine Derivate: Molekül-und Kristallstruktur von S 6 N 4  2+  (FeCl 4  — ) 2  / S 4 N 4  and its Derivatives: Molecular and Crystal Structure of S e N 4  2+  (FeCl 4  - ) 2