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Reaction of dichlorophenylarsane complexes with acetylacetone gives 1,3,2-dioxa arsorine systems, in which both chlorine functions are substituted by the oxygen atoms of one acetylacetone moiety bonded in its diene diol form. Properties and spectra of (CO) 5 CrAsPh(C 5 H 6 O 2 ) and η 5 -C 5 H 5 (CO) 2 MnAsPh(C 5 H 6 O 2 ) are described; the structure of the (CO) 5 Cr complex was established by an X-ray analysis.

zeitschrift für naturforschung b

Acetylaceton als Dien-Diolat-Ligand in 6-Methyl-4-methylen-2-phenyl-4H-1.3.2-dioxa-arsorin- Übergangsmetallkomplexen / Acetylacetone as a Diene Diol Ligand in 6-Methyl-4-methylen-2-phenyl-4H-1,3,2-dioxa-arsorine Transition Metal Complexes