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Interaction of o-phenylenediamine with 1,4-Bis-(ethoxycarbonyl)-2,5-diamino-1,4-cyclo-hexadiene (1) gave 2, which cyclised to the hexahydrobenzodiazepinone (3). On the other hand, interaction of 1 with o-aminophenol, gave compound 4 which on treatment with polyphosphoric acid gave the tetrahydrobis-benzooxazepinone (11). Treatment of 1 with phenylisothiocyanate and formamide afforded the dithiopyrimidoquinazolinone (8) and the tetrahydropyrimidoquinazolinone (9), while the interaction of 1 with benzenesulphonyl-chloride gave dibenzenesulphonamido-cyclohexadiene dicarboxylate (10). The structure of these compounds was established by chemical and spectroscopic methods.

Synthesis of Some Diazepinones, Oxazepinones, Pyrimidoquinazolinones and Related Compounds from 1,4-Bis(ethoxycarbonyl)-2,5-diamino-1,4-cyclohexadiene