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The chloro-tris(carbonylmetalato)tin(IV) compounds, listed in Table I, are obtained by the reaction of TlCo(CO) 4  or Tl[Mn(CO) 5 ] 3  with the dichloro(carbonylmetalato)tin(IV) complexes Cl 2 Sn[M(CO) 5 ] 2  (M = Mn, Re), Cl 2 Sn[Fe(CO) 2 Cp] 2 , Cl 2 Sn[Cr(CO) 3 Cp][Mn(CO) 5 ] and Cl 2 Sn[Cr(CO) 3 Cp][Fe(CO) 2 Cp] in the molar ratio 1:1. Chloro-tris(carbonylmetalato)- tin(TV) compounds of the same type are also formed by treatment of TlCo(CO) 4  with the trichloro(carbonylmetalato)tin(IV) complexes in the molar ratio 2 : 1. The new compounds are characterized by their analyses, mass, IR and FIR spectra. The X-ray analysis of ClSn[Fe(CO) 2 Cp] 2 [Co(CO) 4 ] (space group P2 1 /c) confirms the presence of 3 carbonyl - metalato groups attached to tin.

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Über die Darstellung und Eigenschaften neuer Chloro-tris(carbonylmetaIIato)-zinn(IV)-Komplexe und die Kristallstruktur von ClSn[Fe(CO) 2 Cp] 2 [Co(CO) 4 ]. Synthesis and Properties of New Chloro Tris(carbonylmetalato) Tin(IV) Complexes and the X-ray Structure Analysis of ClSn[Fe(CO) 2 Cp] 2 [Co(CO) 4 ]