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The hitherto unknown title compounds were prepared by a disproportionation reaction starting from elementary rubidium and indium monosulfide. Rb 4 ln 2 S 5  crystallizes in the triclinic system (P1̄) with the lattice constants a = 931.7(2); b = 1097.6(3);c = 761.2(2)pm; a = 111.32°(2); β = 94.70°(2); γ = 103.70°(2) (Z = 2) and Rb 6 In 2 S 6  in the monoclinic system (C2/m) with the lattice constants a = 895.3(2); b = 1356.9(2); c = 791.8(2) pm; β = 101.53°(2) (Z = 2). The quasi molecular [In 2 Se 6 ] 6-  group which is isoelectronic with the gas phase molecule In 2 Cl 6  consists of two edge sharing InS 4  tetrahedra and is the basic unit of Rb 6 ln 2 S 6  as well as of Rb 6 In 2 S 6 . The formation process, structural relationships between the two compounds and their possible role in the phase diagram of the components Rb 2 S and In 2 S 3  are discussed.

zeitschrift für naturforschung b

Rb 6 In 2 S 6  und Rb 4 In 2 S 5 , zwei neue Thioindate mit isolierten und verknüpften [In 2 S 6 ] 6-  Anionen / Rb 6 In 2 Se 6  and Rb 4 ln 2 S 5 , Two NEW Thioindates with Isolated and Connected [In 2 S 6 ] 6-  Anions Respectively