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The title compound is prepared by treating ReNCL with excess POCl 3 . The complex is isotypic with the corresponding tungsten complex [WNCl 3  · POCl 3 ] 4  · 2 POCl 3 . The structure consists of Re 4 N 4  eight-membered rings with alternating Re ≡ N-Re bonds. The IR spectrum was recorded and assigned.

zeitschrift für naturforschung b

Notizen: Darstellung, IR-Spektrum und Kristalldaten von [ReNCl 3  · POCl 3 ] 4  · 2POCl 3 /Preparation, IR Spectrum and Crystallographic Data of [ReNCL · POCl 3 ] 4  · 2 POCl 3