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The title compound (1) was crystallized as free ligand and as its (1 · KSCN) 2  · H 2 O complex. Crystallographic data are, for the former: space group C 2/c, a = 31.110(9), b = 4.608(4), c = 17.188(6) Å, β = 105.27(8)°, Z = 2, D m  = 1.25 gem -3 ; for the latter: space group P2 1 , a = 11.044(3), b = 18.310(4), c = 14.485(4) Å, β = 97.49(2)°, Z = 4, Dm = 1.27 gem -3 . Crystal structures were solved by direct methods using X-ray diffraktometer data and least squares refinements converged at 10.8% for 1 and at 7.6% for (1 · KSCN)2 · H2O.

Structural Change of a Line ar Polyether upon Complex Formation. 1.11-Bis(2-acetylaminophenoxy)-3.6.9-trioxaundecane and its KSCN Complex a