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Cl 3 VNI crystallizes isotypically with Cl 3 VNCI in the triclinic space group P1̄. The crystals contain dimeric units which are formed via chlorine bridges. The VNI group is linear with an sp-hybridized nitrogen and a V-N triple bond, (angle VNI = 163°, V-N = 165 pm, N-I = 193 pm). A short contact distance of 307 pm between the I atom and a neighbouring Cl atom is observed.

Die Kristallstmktiir des Iodnitren-Komplexes Cl 3 V ≡ N-I / Crystal Structure of the Iodonitrene Complex, Cl 3 V≡N-I