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The title compound was prepared by reaction of AgNO 3 , P(C 6 H 5 ) 3  and (NH 4 ) 2 WS 4  in a dichloromethane/water system. The crystal structure was determined from single crystal X-ray diffraction data (monoclinic, space group P2 1 /c, with a = 1811,1(2), b = 1735.6(2), c = 1779,7(2) pm, β = 95,02(1)°, V = 5572,7 · 10 6  pm 3 , Z = 4). The compound contains a tetradentate WS 4  2-  ligand and two silver atoms, having a tetrahedral and trigonal planar coordination.

zeitschrift für naturforschung b

Darstellung und Kristallstruktur von (PPh 3 ) 3 Ag 2 WS 4 , einem neuartigen Dreikern-Komplex mit tetraedrisch und trigonal planar koordinierten Ag-Atomen / Preparation and Crystal Structure of (PPh 3 ) 3 Ag 2 WS 4 , a Novel Trinuclear Complex with Tetrahedral and Trigonal Planar Coordination of the Ag Atoms