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The covalent carbamoyl compounds M(CO) 2 (PR 3 ) 2 (Hal)(CONH 2 ) (M = Fe, Ru, Os; Hal = Cl, Br; R = Ph, Cyclohexyl) and Os(CO)(NO)(PPh 3 ) 2 (CONH 2 ) are formed by the reactions of the cationic complexes [M(CO) 3 (PR 3 ) 2 (Hal)] +  and [Os(CO) 2 (NO)(PPh 3 ) 2 ] +  with liquid NH 3  between -75 and -40 °C.

zeitschrift für naturforschung b

Über neue Carbamoyl-carbonyl-Komplexe des Eisens, Rutheniums und Osmiums [1] / About New Carbamoyl Carbonyl Complexes of Iron, Ruthenium and Osmium [1]