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(R 3 P) 2 NiCl 2  and LiP(SiMe 3 ) 2  react in a complex reaction sequence finally yielding (R 3 P) 2 Ni(PSiMe 3 ) 2  (5), containing a three-membered PNiP ring system, and [R 3 PNiP(SiMe 3 ) 2 ] 2  (6), containing a (PNi) 2  four-membered ring system with a nickel-nickel bond, respectively. NMR data are reported.

zeitschrift für naturforschung b

Übergangsmetallphosphidokomplexe, III [1] Neuartige Nickel-Phosphor-Drei-und Vierringkomplexe / Transition Metal Phosphido Complexes, III [1] Novel Nickel Phosphorus Three-, and Four-Membered Ring Complexes