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(CH 3 ) 3  Pconvertsa,a,w-dibromopentaneand-hexane into w-bromoalkyltrimethylphos-phonium bromides,which undergo a cyclizationon treatment with NaNH 2  in tetrahydro-furane to form the cyclopentyl-and cyclohexyl-dimethyl-methylenephosphoranes 4 and 5. From the bis-phosphonium salt(CH 3 ) 3 P(CH 2 ) 6 P(CH 3 ) 3  2⊕  2Br ⊖  the difunctional bis-ylide CH 2 =(CH 3 ) 2 P(CH 2 ) 6 P(CH 3 ) 2 =CH 2 (7)is obtained. The ylide 4 was characterized by the crystalline metallocyclic Au(I)derivative 8.7 forms a polymeric gold complex.

zeitschrift für naturforschung b

Cyclopentyl-und Cyclohexyl-dimethyl-methylen-phosphoran aus w-Haloalkyl-trimethylphosphonium-salzen. Goldkomplexe mono-und difunktioneller Ylide / Cyclopentyl-and Cyclohexyl-dimethyl-methylene-phosphoranes from w-Haloalkyl-trimethylphosphonium Salts. Gold Complexes of Mono-and Difunctional Ylides