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Cis-dicarbonyl complexes of Fe(II) with o-benzenedithiolate and o-methylthiobenzenethiolate ligands react with PMe 3  yielding [Fe(CO) 2 (PMe 3 ) 2 (C 6 H 4 S 2 )] and [Fe(CO)(PMe 3 )(CH 3 S-C 6 H 4 -S) 2 ], respectively. The reaction of [Fe(CH 3 S-C 6 H 4 -S) 2 ], accessible only in solution, with PMe 3  affords the labile [Fe(PMe 3 ) 2 (CH 3 S-C 6 H 4 -S) 2 ], which with CO rapidly yields the monocarbonyl complex [Fe(CO)(PMe 3 )(CH 3 S-C 6 H 4 -S 2 )]. The anion [Fe(CO) 2 (C 6 H 4 S 2 ) 2 ] 2- , hitherto accessible in solution only, could be precipitated in the presence of NaBH 4  as (NMe 4 ) 2 [Fe(CO) 2 (C 6 H 4 S 2 ) 2 ]

zeitschrift für naturforschung b

Synthese und Reaktionen von Eisen-Schwefel-Komplexen mit CO- und P(CH 3 ) 3 -Liganden [1] / Synthesis and Reactions of Iron Sulfur Complexes with CO and P(CH 3 ) 3  Ligands