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NiC 6 H 14 N 8 O 6  is obtained in a dimeric form, bridged by oxime O atoms, as a by-product during the preparation of bis(malonenamide-oximato)nickel(II). It crystallizes in the mono-clinic space group P2 1 /c with a = 10.053(3), b = 9.338(3), c = 13.392(3) Å, β = 92.09°. The structure was solved by direct and Fourier methods and refined by least squares to R = 0.071 for 2462 intensities.

Dimeres Aquo(malonenamidoximato)-(2-ketomalonenamidoximato)-nickel(II) / Dimeric Aquo(malonenamide-oximato)- (2-ketomalonenamide-oximato)-nickel(II)