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A series of new planar bis(α,β-dionedioximato) metal(II) complexes of the ions Ni(II), Pd(II), Pt(II)using unsymmetrically substituted glyoximes as ligands are reported. Typical ligands being unsymmetrically substituted benzildioximes, phenylglyoxime or butan-1,2-dionedioxime.The solid state properties and in some cases the X-ray data suggest, that most of the isolated complexes crystallize in columnar stacks. Compared with the known symmetrical derivatives the solubility of the isolated neutral compounds in organic solvents like ethanol, chloroform or 1,2-dichlorobenzene is highly increased. Most of the compounds can therefore be obtained in good crystalline form. The good solubility is an advantage in the efforts to extend the polarizable ligand system of the complexes.

zeitschrift für naturforschung b

Planare Komplexe von unsymmetrisch substituierten Alkyl- und Aryl-α.β-diondioximen mit den Ionen Nickel(II), Palladium(II) und Platin(II) / Planar Complexes of Unsymmetrically Substituted Alkyl and Aryl-1,2-dionedioximes with the Ions Nickel(II), Palladium(II) and Platinum(II)