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η 4  (1,2-Di-tert-butyl-3,4,5,6-tetramethylbenzo-cyclobutadiene)tricarbonyliron (2) is prepared by reaction of the respective free benzocyclo-butadiene (1) and nonacarbonyl-diiron at room temperature. X-ray data of the free and complexed ligand are compared.

Strukturwandel eines Benzocyclobutadiens bei seiner Komplettierung/Structural Change of a Benzocyclobutadiene by Complexation