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Tri-tert-butylchlorosilane reacts with potassium pseudohalides in the presence of catalytic amounts of the crown ether 18-crown-6 to give the tri-tert-butylsilicon pseudo-halides (t-C 4 H 9 ) 3 SiX (X = CN, NCO, NCS, N 3 ) in good yields. These new compounds are characterized by IR,  1 H NMR, and mass spectra. In the absence of the crown ether no reaction occurs. Treating tri-tert-butylsilane with AgX (X = CN, SCN) gives the silicon pseudohalides in low yields.

zeitschrift für naturforschung b

Siliciumverbindungen mit starken intramolekularen sterischen Wechselwirkungen, VII [1]. Tri-tert-butylsiliciumpseudohalogenide / Silicon Compounds with Strong Intramolecular Steric Interactions, VII [1]. Tri-tert-butylsilicon Pseudohalides