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Various homogeneous metalate(O) complexes are synthesized with [SnCl 3 ] -as a ligand. Complexes of the type [M(SnCl 3 ) 6 ] 6-  are prepared from [M(CO) 3 (SnCl 3 ) 3 ] 3- (M = Cr, Mo, W) in nitromethane. [Fe(SnCl 3 ) 5 ] 5-  is formed by UV irradiation of [Fe(CO) 4 SnCl 3 ] -  in aceto-nitrile. [M(SnCl 3 ) 4 ] 4 -(M = Ni, Pd, Pt) anions are synthesized by thermal substitution reactions with Ni(CO) 4 , Pd(PF 3 ) 4 , and Pt(PF 3 ) 4 . All metalate(O) ions are isolated as salts with the [N(C 2 H 5 ) 4 ] +  cation and characterized by IR spectra and  119m Sn-Mössbauer spectra as well as by analysis.

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Metallkomplexe mit anionischen Liganden von Elementen der 4. Hauptgruppe, XI Homogene Trichlorstannidometallat(O)-Komplexe der 6. und 8. Nebengruppe/Metal Complexes with Anionic Ligands of Elements of the Main Group IV, XI Homogenous Trichlorostannido Metalate(O) Complexes of the Transition Groups VI and VIII