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The azidophosphine complexes cis-Mo(CO) 4 (R 2 PN 3 ) 2  (R = Me, Ph) may be obtained by nucleophilic displacement reactions of chlorine by azide ion in complexes cis-Mo(CO) 4 (R 2 PCl) 2 . The thermal decomposition and Staudinger reactions were studied. Silylation of NH- or NH 2 -functional groups in aminophosphine and hydrazinophosphine complexes with Me 3 SiCl, Me 2 SiCl 2  or Me 2 SiCl-SiClMe 2  leads to a series of monodentate or bidentate silylaminophosphine complexes, e.g. (CO) 4 Mo(R 2 PNHSiMe 3 ) 2 , (CO) 4 Mo-(R 2 PNH) 2 SiMe 2 , (CO) 4 Mo(R 2 PNH) 2 (SiMe 2 ) 2 , (CO) 4 Mo[R 2 PN(SiMe 3 )(SiMe 3 )NPR 2 ] or (CO) 4 Mo[R 2 P-N(SiMe 3 )SiMe 2 -SiMe 2 -N(SiMe 3 )PR 2 ].

zeitschrift für naturforschung b

Reaktionen koordinierter Liganden, V / Reactions of Coordinated Ligands, V: Reaktionen an funktionellen Gruppen von Azido-, Amino- und Hydrazidophosphinkomplexen des Typs cis-Mo(CO) 4 L 2  /  Reactions at Functional Groups of Azido-, Amino-, and Hydrazidophosphine Complexes of the Type cis-Mo(CO) 4 L 2