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TlPbI 3 , which is prepared from PbI 2  and TlI by the BRIDGMAN-STOCKBARGER technique, crystallizes in the orthorhombic space group Cmcm with a = 4.625(2), b = 14.885(4), c = 11.857(4) Å, Z = 4. Tl 4 PbI 6  is prepared from PbI 2  and TlI in n/10 HCl under hydrothermal conditions. The compound crystallizes in the orthorhombic space group Pbam with a = 19.117(9), b = 9.877(9), c = 4.586(4) Å, Z = 2. Both structures were solved by direct methods. Both compounds contain PbI 6 -octahedra which are found in PbI 2  and the structural elements of TlI

Die Kristallstrukturen von TIPbI 3 und Tl 4 PbI 6 / The Crystal Structures of TlPbI 3 and Tl 4 PbI 6