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29 Si,  31 P and, in part,  13 C NMR data are reported for N-trimethylsilyl-triorganophosphine imines as well as some siliconsubstituted methoxy and chloro derivatives. The spin-spin splitting pattern of the  29 Si{ 1 H} spectra is discussed for disilanes of the type (RR′R″P=N-SiMe 2 -) 2 . A qualitative interpretation of  29 Si chemical shifts is preferably being based on hyperconjugation rather than a (p-d)n bonding mechanism. The preparation of a series of bis(phosphinimino)silanes and 1,2-bis(phosphinimino)disilanes is described.

zeitschrift für naturforschung b

29 Si-,  31 P- und  13 C-Kernresonanzuntersuchungen an N-silylierten Triorganophosphiniminen / Silicon-29, Phosphorus-31, and Carbon-13 Nuclear Magnetic Resonance Investigations of N-Silylated Triorganophosphine Imines