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Quantitative kinetic results of the intermediates and end products of the formose reaction are obtained for the first time by the application of high pressure liquid chromatography. A mechanism for the secondary reaction step of the formose reaction in the presence of excess formaldehyde is derived from these results : Formaldehyde adds successively to intermediates and the formation of xylose is highly favoured. All results are characteristic for typical aldol-type reactions. Almost no cleavage of the intermediate and end products is observed.

zeitschrift für naturforschung b

Formose-Reaktion, I Kinetik und Mechanismus der Sekundärreaktionen bei Anwesenheit von Formaldehyd / Formose Reaction, I Kinetics and Mechanism of the Secondary Reaction Step in the Presence of Formaldehyde