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The spin-labeled (1-oxyl-2,2,6,6-tetramethyl-4-piperidyl)-phenyl imidazole-1-phosphonate (4) was used to prepare (1-oxyl-2,2,6,6-tetramethyl-4-piperidyl)phenyl N-alkyl and N-aryl phosphoroamidates (8) in yields generally exceeding 70%.

Preparation of Spin-Labeled Phosphoroamidates in High Yield Using Imidazole as the Transfer Agent